Dear Enduser,
Please access the website
http://www.practicingoilanalysis.com and reference the article;
"Grease Analysis - Monitoring Grease Servicability and Bearing Condition" by
Bill Herguth, Herguth Laboratories
I am not sure if it will give you an answer cast in stone but will point you in the right direction.
Here are some quotes out of the article to wet your appetite;
"...Thermal Gravimetric Analysis (TGA). TGA analysis measures the mass of a substance in relationship to temperature and is used to determine the loss of material with increasing temperature. The analysis can be carried out in an inert atmosphere such as nitrogen or a reactive atmosphere such as oxygen. Typically, a few milligrams of the sample is weighed and heated under controlled conditions. The weight loss at specific temperatures allows the technician to evaluate the oil/gelling agent ratio as compared to new (unused grease), as well as the presence of volatile compounds such as water, allowing any significant change in gelling agent chemistry to be determined..."
and
"...Rheology is the study of the deformation and/or flow of matter when it is subjected to strain, temperature and time. A rheometer only requires a few grams of sample to perform the analysis, yielding much more information than the cone penetration or the apparent viscosity measurements. This makes the rheology measurement an ideal test for small amounts of used grease..."
Have fun.